COL ICSD Collection Code 200146 DATE Recorded Jan 1, 1980; updated May 26, 1987 NAME Hexapotassium hexaniobium tetragermanium oxide FORM K6 Nb6 Ge4 O26 = Ge4 K6 Nb6 O26 TITL Etude du comportement du germanium dans les structures a tunnels de section pentagonale: Les silicogermanates K6 Nb6 Gex Si4-x O26 REF Revue de Chimie Minerale RVCMA 14 (1977) 311-317 AUT Choisnet J, Nguyen˙N, Raveau˙B CELL a=9.188 b=9.188 c=8.123 à=90.0 á=90.0 ç=120.0 V=593.9 Z=1 SGR P -6 2 m (189) - hexagonal CLAS -6m2 (Hermann-Mauguin) - D3h (Schoenflies) PRS hP42 ANX A2B3C3X13 PARM Atom__No OxStat Wyck ---X--- ---Y--- ---Z--- -SOF- K 1 1.000 3g 0.61 0. 1/2 K 2 1.000 3f 0.599 0. 0. Ge 1 4.000 4h 1/3 2/3 0.219 Nb 1 5.000 6i 0.232 0. 0.239 O 1 -2.000 2c 1/3 2/3 0. O 2 -2.000 3f 0.228 0. 0. O 3 -2.000 6i 0.831 0. 0.292 O 4 -2.000 12l 0.478 0.166 0.28 O 5 -2.000 3g 0.256 0. 1/2 WYCK l i2 h g2 f2 c ITF K 1 B=2.9 ITF K 2 B=0.3 ITF Ge 1 B=2.4 ITF Nb 1 B=0.6 ITF O 1 B=0.1 ITF O 2 B=0.2 ITF O 3 B=0.2 ITF O 4 B=0.2 ITF O 5 B=2.9 RVAL 0.088 TEST At least one temperature factor is implausible or meaningless but agrees with the value given in the paper. (Code 52)