COL  ICSD Collection Code 80052
 DATE Recorded Oct 14, 1996
 NAME Tetralanthanum nonatitanium oxide
 FORM La4 Ti9 O24
      = La4 O24 Ti9
 TITL The structure of La4 Ti9 O24 from synchrotron X-ray powder 
      diffraction
 REF  Journal of Physics and Chemistry of Solids
      JPCSA 56 (1995) 1297-1303  Issue 10
 AUT  Morris R E, Owen’J’J, Cheetham’A’K
 CELL a=14.146 b=35.527 c=14.579 ą=90.0 į=90.0 ē=90.0
      V=7326.9 Z=16
 SGR  F d d d Z     (70) - orthorhombic
 CLAS mmm   (Hermann-Mauguin) - D2h (Schoenflies)
 PRS  oF592
 ANX  A4B9X24
 PARM Atom__No OxStat  Wyck ---X--- ---Y--- ---Z---  -SOF-
      La     1  3.000   16f  3/8     0.01719 3/8
      La     2  3.000   16f  5/8     0.99347 1/8
      La     3  3.000   32h  0.2812  0.12268 0.27303
      Ti     1  4.000   32h  0.0218  0.08225 0.7525
      Ti     2  4.000   32h  0.1333  0.95527 0.3725
      Ti     3  4.000   16f  5/8     0.08159 5/8
      Ti     4  4.000   32h  0.2358  0.08139 0.7559
      Ti     5  4.000   32h  0.6213  0.03715 0.8466
      O      1 -2.000   32h  0.0152 -0.0815  0.8898
      O      2 -2.000   16g  1/8     1/8     0.0261
      O      3 -2.000   32h  0.1184 -0.0568  0.26
      O      4 -2.000   32h  0.0323 -0.0078  0.3551
      O      5 -2.000   32h  0.2061 -0.0052  0.3736
      O      6 -2.000   32h  0.1151  0.041   0.0334
      O      7 -2.000   16g  1/8     5/8     0.9976
      O      8 -2.000   32h  0.1203  0.0487  0.4971
      O      9 -2.000   32h  0.5144  0.1781  0.8789
      O     10 -2.000   32h  0.9554  0.1296  0.7897
      O     11 -2.000   32h  0.4017  0.0482  0.0014
      O     12 -2.000   32h  0.5261  0.0668  0.8486
      O     13 -2.000   32h  0.2573  0.0839  0.6205
 WYCK h16 g2 f3
 ITF  La  1   U=0.0320(13)
 ITF  La  2   U=0.0365(14)
 ITF  La  3   U=0.0366(9)
 ITF  Ti  1   U=0.0282(32)
 ITF  Ti  2   U=0.0335(21)
 ITF  Ti  3   U=0.0397(34)
 ITF  Ti  4   U=0.0461(41)
 ITF  Ti  5   U=0.0273(25)
 ITF  O   1   U=0.039(12)
 ITF  O   2   U=0.010(8)
 ITF  O   3   U=0.036(9)
 ITF  O   4   U=0.018(9)
 ITF  O   5   U=0.003(6)
 ITF  O   6   U=0.037(10)
 ITF  O   7   U=0.038(13)
 ITF  O   8   U=0.006(7)
 ITF  O   9   U=0.011(7)
 ITF  O  10   U=0.007(6)
 ITF  O  11   U=0.058(14)
 ITF  O  12   U=0.018(10)
 ITF  O  13   U=0.025(8)
 REM  SNP (synchroton radiation, powder diffraction)
 REM  RVP
 RVAL 0.152