$ RUN RUNFILE NBS*QUANT84-RUNFIL Revision Date: 29 FEB 1984 Calculates Irel and/or RIR and/or I/Io and/or Quantitative Analysis RUN files Written by R. L. Snyder and C. R. Hubbard Run on 5-AUG-8 at 00:40:12 Select the option for the type of RUN desired: 1 - Create a RUN file for the Internal Standard Method 2 - Create a RUN file for the Intensity Ratio Method 3 - Compute RIR's from the rel I's on the files 4 - Compute Relative Intensities 5 - Compute RIR's from computed rel I's 1 Select Output Mode Desired: (Output is 132 characters wide) 1 - causes output to be put on the interactive terminal. newname - causes output to go to the named file. - causes output to go to a file named RUNFIL.LIS. Enter the output destination: 1 Select a print control option (I1): 0 = Full listing of data files 1 = Heading on first data file only 2 = Data file titles only 2 Enter weighting choice: 0 for counting statistical weights 1 for unit weights 0 Input all the files for calibration phase number 1 Enter a blank for the requested file name after the last file for this phase has been processed Enter name for file # 1 CR065D Title: 6GMQTZ.-4GMS SI. FOR INTERNAL STANDARD JOHN J. SIMMINS The rest of this physical file will be skipped using only up to set 1 Enter name for file # 2 CR067D Title: 60%QTZ-40%SI; SPRAYDRIED; INTERNAL STANDARD JOHN J. SIMMINS Enter name for file # 4 Relative intensity analysis: The following line(s) will be used in scaling ln Phase h k l Method 2 QUARTZ 1 0 1 INTEGRT 4 SILICN 1 1 1 INTEGRT File analyte line Irel=100 line relative Standard Root mean Number of # Phase h k l Name h k l Intensity Deviation square dev. measurments 1 QUARTZ 1 0 0 QUARTZ 1 0 1 17.098 0.026 2 QUARTZ 1 0 0 QUARTZ 1 0 1 17.611 0.028 3 QUARTZ 1 0 0 QUARTZ 1 0 1 18.345 0.029 QUARTZ 1 0 0 Wt Mean 17.646 0.016 0.361 3 File analyte line Irel=100 line relative Standard Root mean Number of # Phase h k l Name h k l Intensity Deviation square dev. measurments 1 QUARTZ 1 0 1 QUARTZ 1 0 1 100.000 0.136 2 QUARTZ 1 0 1 QUARTZ 1 0 1 100.000 0.142 3 QUARTZ 1 0 1 QUARTZ 1 0 1 100.000 0.142 QUARTZ 1 0 1 Wt Mean 100.000 0.081 0.000 3 File analyte line Irel=100 line relative Standard Root mean Number of # Phase h k l Name h k l Intensity Deviation square dev. measurments 1 QUARTZ 1 0 1 QUARTZ 1 0 1 93.294 0.106 2 QUARTZ 1 0 1 QUARTZ 1 0 1 94.893 0.111 3 QUARTZ 1 0 1 QUARTZ 1 0 1 92.781 0.109 QUARTZ 1 0 1 Wt Mean 93.634 0.063 0.627 3 File analyte line Irel=100 line relative Standard Root mean Number of # Phase h k l Name h k l Intensity Deviation square dev. measurments 1 QUARTZ 1 1 1 QUARTZ 1 0 1 2.949 0.045 2 QUARTZ 1 1 1 QUARTZ 1 0 1 3.044 0.048 3 QUARTZ 1 1 1 QUARTZ 1 0 1 3.051 0.048 QUARTZ 1 1 1 Wt Mean 3.012 0.027 0.033 3 File analyte line Irel=100 line relative Standard Root mean Number of # Phase h k l Name h k l Intensity Deviation square dev. measurments 1 QUARTZ 2 0 0 QUARTZ 1 0 1 4.804 0.040 2 QUARTZ 2 0 0 QUARTZ 1 0 1 4.906 0.043 3 QUARTZ 2 0 0 QUARTZ 1 0 1 4.792 0.043 QUARTZ 2 0 0 Wt Mean 4.833 0.024 0.036 3 File analyte line Irel=100 line relative Standard Root mean Number of # Phase h k l Name h k l Intensity Deviation square dev. measurments 1 SILICN 1 1 1 SILICN 1 1 1 100.000 0.155 2 SILICN 1 1 1 SILICN 1 1 1 100.000 0.164 3 SILICN 1 1 1 SILICN 1 1 1 100.000 0.165 SILICN 1 1 1 Wt Mean 100.000 0.093 0.000 3 File analyte line Irel=100 line relative Standard Root mean Number of # Phase h k l Name h k l Intensity Deviation square dev. measurments 1 SILICN 3 1 1 SILICN 1 1 1 29.307 0.106 2 SILICN 3 1 1 SILICN 1 1 1 31.511 0.115 3 SILICN 3 1 1 SILICN 1 1 1 31.551 0.117 SILICN 3 1 1 Wt Mean 30.698 0.065 0.761 3 File analyte line Irel=100 line relative Standard Root mean Number of # Phase h k l Name h k l Intensity Deviation square dev. measurments 1 SILICN 3 1 1 SILICN 1 1 1 22.084 0.049 2 SILICN 3 1 1 SILICN 1 1 1 22.725 0.052 3 SILICN 3 1 1 SILICN 1 1 1 22.837 0.053 SILICN 3 1 1 Wt Mean 22.525 0.030 0.239 3 Summary of relative intensities Phase h k l Method Intensity e.s.d. rms dev # QUARTZ 1 0 0 INTEGRT 17.646 0.016 0.361 3 QUARTZ 1 0 1 INTEGRT 100.000 0.081 0.000 3 QUARTZ 1 0 1 PEAK HT 93.634 0.063 0.627 3 QUARTZ 1 1 1 INTEGRT 3.012 0.027 0.033 3 QUARTZ 2 0 0 INTEGRT 4.833 0.024 0.036 3 Phase h k l Method Intensity e.s.d. rms dev # SILICN 1 1 1 INTEGRT 100.000 0.093 0.000 3 SILICN 3 1 1 INTEGRT 30.698 0.065 0.761 3 SILICN 3 1 1 PEAK HT 22.525 0.030 0.239 3 RIR Calibration for quantitative analysis by the internal standard method ***** Line by line RIR analysis ***** File Analyte Line Standard Line RIR Standard Root Mean Number of Degrees of # Phase h k l Name h k l Constant Deviation square dev. measurments freedom 1 QUARTZ 1 0 0 SILICN 1 1 1 0.8798 0.0018 2 QUARTZ 1 0 0 SILICN 1 1 1 0.9287 0.0020 3 QUARTZ 1 0 0 SILICN 1 1 1 0.9865 0.0021 QUARTZ 1 0 0 Wt Mean 1 1 1 0.9268 0.0011 0.0307 3 2 File Analyte Line Standard Line RIR Standard Root Mean Number of Degrees of # Phase h k l Name h k l Constant Deviation square dev. measurments freedom 1 QUARTZ 1 0 1 SILICN 1 1 1 0.9080 0.0017 2 QUARTZ 1 0 1 SILICN 1 1 1 0.9306 0.0018 3 QUARTZ 1 0 1 SILICN 1 1 1 0.9489 0.0019 QUARTZ 1 0 1 Wt Mean 1 1 1 0.9281 0.0010 0.0119 3 2 File Analyte Line Standard Line RIR Standard Root Mean Number of Degrees of # Phase h k l Name h k l Constant Deviation square dev. measurments freedom 1 QUARTZ 1 0 1 SILICN 1 1 1 0.9047 0.0015 2 QUARTZ 1 0 1 SILICN 1 1 1 0.9431 0.0016 3 QUARTZ 1 0 1 SILICN 1 1 1 0.9403 0.0016 QUARTZ 1 0 1 Wt Mean 1 1 1 0.9282 0.0009 0.0126 3 2 File Analyte Line Standard Line RIR Standard Root Mean Number of Degrees of # Phase h k l Name h k l Constant Deviation square dev. measurments freedom 1 QUARTZ 1 1 1 SILICN 1 1 1 0.8890 0.0159 2 QUARTZ 1 1 1 SILICN 1 1 1 0.9405 0.0171 3 QUARTZ 1 1 1 SILICN 1 1 1 0.9611 0.0176 QUARTZ 1 1 1 Wt Mean 1 1 1 0.9276 0.0097 0.0218 3 2 File Analyte Line Standard Line RIR Standard Root Mean Number of Degrees of # Phase h k l Name h k l Constant Deviation square dev. measurments freedom 1 QUARTZ 2 0 0 SILICN 1 1 1 0.9026 0.0088 2 QUARTZ 2 0 0 SILICN 1 1 1 0.9447 0.0095 3 QUARTZ 2 0 0 SILICN 1 1 1 0.9409 0.0097 QUARTZ 2 0 0 Wt Mean 1 1 1 0.9279 0.0054 0.0138 3 2 File Analyte Line Standard Line RIR Standard Root Mean Number of Degrees of # Phase h k l Name h k l Constant Deviation square dev. measurments freedom 1 QUARTZ 1 0 0 SILICN 3 1 1 0.9216 0.0040 2 QUARTZ 1 0 0 SILICN 3 1 1 0.9047 0.0039 3 QUARTZ 1 0 0 SILICN 3 1 1 0.9598 0.0042 QUARTZ 1 0 0 Wt Mean 3 1 1 0.9274 0.0023 0.0160 3 2 File Analyte Line Standard Line RIR Standard Root Mean Number of Degrees of # Phase h k l Name h k l Constant Deviation square dev. measurments freedom 1 QUARTZ 1 0 1 SILICN 3 1 1 0.9511 0.0040 2 QUARTZ 1 0 1 SILICN 3 1 1 0.9066 0.0039 3 QUARTZ 1 0 1 SILICN 3 1 1 0.9233 0.0040 QUARTZ 1 0 1 Wt Mean 3 1 1 0.9264 0.0023 0.0130 3 2 File Analyte Line Standard Line RIR Standard Root Mean Number of Degrees of # Phase h k l Name h k l Constant Deviation square dev. measurments freedom 1 QUARTZ 1 0 1 SILICN 3 1 1 0.9476 0.0039 2 QUARTZ 1 0 1 SILICN 3 1 1 0.9187 0.0038 3 QUARTZ 1 0 1 SILICN 3 1 1 0.9149 0.0038 QUARTZ 1 0 1 Wt Mean 3 1 1 0.9268 0.0022 0.0103 3 2 File Analyte Line Standard Line RIR Standard Root Mean Number of Degrees of # Phase h k l Name h k l Constant Deviation square dev. measurments freedom 1 QUARTZ 1 1 1 SILICN 3 1 1 0.9312 0.0170 2 QUARTZ 1 1 1 SILICN 3 1 1 0.9162 0.0170 3 QUARTZ 1 1 1 SILICN 3 1 1 0.9351 0.0174 QUARTZ 1 1 1 Wt Mean 3 1 1 0.9274 0.0099 0.0058 3 2 File Analyte Line Standard Line RIR Standard Root Mean Number of Degrees of # Phase h k l Name h k l Constant Deviation square dev. measurments freedom 1 QUARTZ 2 0 0 SILICN 3 1 1 0.9454 0.0099 2 QUARTZ 2 0 0 SILICN 3 1 1 0.9203 0.0099 3 QUARTZ 2 0 0 SILICN 3 1 1 0.9155 0.0100 QUARTZ 2 0 0 Wt Mean 3 1 1 0.9271 0.0057 0.0093 3 2 File Analyte Line Standard Line RIR Standard Root Mean Number of Degrees of # Phase h k l Name h k l Constant Deviation square dev. measurments freedom 1 QUARTZ 1 0 0 SILICN 3 1 1 0.8974 0.0025 2 QUARTZ 1 0 0 SILICN 3 1 1 0.9206 0.0026 3 QUARTZ 1 0 0 SILICN 3 1 1 0.9730 0.0028 QUARTZ 1 0 0 Wt Mean 3 1 1 0.9278 0.0015 0.0220 3 2 File Analyte Line Standard Line RIR Standard Root Mean Number of Degrees of # Phase h k l Name h k l Constant Deviation square dev. measurments freedom 1 QUARTZ 1 0 1 SILICN 3 1 1 0.9261 0.0025 2 QUARTZ 1 0 1 SILICN 3 1 1 0.9224 0.0025 3 QUARTZ 1 0 1 SILICN 3 1 1 0.9360 0.0026 QUARTZ 1 0 1 Wt Mean 3 1 1 0.9280 0.0014 0.0040 3 2 File Analyte Line Standard Line RIR Standard Root Mean Number of Degrees of # Phase h k l Name h k l Constant Deviation square dev. measurments freedom 1 QUARTZ 1 0 1 SILICN 3 1 1 0.9228 0.0023 2 QUARTZ 1 0 1 SILICN 3 1 1 0.9348 0.0024 3 QUARTZ 1 0 1 SILICN 3 1 1 0.9275 0.0024 QUARTZ 1 0 1 Wt Mean 3 1 1 0.9282 0.0014 0.0035 3 2 File Analyte Line Standard Line RIR Standard Root Mean Number of Degrees of # Phase h k l Name h k l Constant Deviation square dev. measurments freedom 1 QUARTZ 1 1 1 SILICN 3 1 1 0.9068 0.0163 2 QUARTZ 1 1 1 SILICN 3 1 1 0.9322 0.0170 3 QUARTZ 1 1 1 SILICN 3 1 1 0.9480 0.0174 QUARTZ 1 1 1 Wt Mean 3 1 1 0.9281 0.0098 0.0121 3 2 File Analyte Line Standard Line RIR Standard Root Mean Number of Degrees of # Phase h k l Name h k l Constant Deviation square dev. measurments freedom 1 QUARTZ 2 0 0 SILICN 3 1 1 0.9206 0.0092 2 QUARTZ 2 0 0 SILICN 3 1 1 0.9364 0.0096 3 QUARTZ 2 0 0 SILICN 3 1 1 0.9281 0.0097 QUARTZ 2 0 0 Wt Mean 3 1 1 0.9281 0.0055 0.0046 3 2 Wt Mean Over the standard lines used: File Analyte Line Standard Line RIR Standard Root Mean Number of Degrees of # Phase h k l Name h k l Constant Deviation square dev. measurments freedom QUARTZ 1 0 0 SILICN all 0.9272 0.0008 0.0169 9 5 QUARTZ 1 0 1 SILICN all 0.9279 0.0008 0.0060 9 6 QUARTZ 1 0 1 SILICN all 0.9281 0.0007 0.0067 9 5 QUARTZ 1 1 1 SILICN all 0.9277 0.0057 0.0094 9 5 QUARTZ 2 0 0 SILICN all 0.9277 0.0032 0.0064 9 5 Overall Wt Mean over all lines for each phase: File Analyte Line Standard Line RIR Standard Root Mean Number of Degrees of # Phase h k l Name h k l Constant Deviation square dev. measurments freedom QUARTZ all SILICN all 0.9277 0.0004 0.0046 45 26 Are files for another calibration phase to be entered? (y/n) Y Input all the files for calibration phase number 2 Enter a blank for the requested file name after the last file for this phase has been processed Enter name for file # 1 CR071D Title: 6GM MULLITE TO 4GM SILICON WITH 0.2 GM PVA THEN SPRAY DRIED CAMDEN HUBBARD Enter name for file # 4 Relative intensity analysis: The following line(s) will be used in scaling ln Phase h k l Method 2 MULITE DOUBLT INTEGRT 4 SILICN 1 1 1 INTEGRT File analyte line Irel=100 line relative Standard Root mean Number of # Phase h k l Name h k l Intensity Deviation square dev. measurments 1 MULITE 1 1 0 MULITE DOUBLT 43.435 0.176 2 MULITE 1 1 0 MULITE DOUBLT 41.582 0.154 3 MULITE 1 1 0 MULITE DOUBLT 44.234 0.161 MULITE 1 1 0 Wt Mean 43.012 0.094 0.814 3 File analyte line Irel=100 line relative Standard Root mean Number of # Phase h k l Name h k l Intensity Deviation square dev. measurments 1 MULITE DOUBLT MULITE DOUBLT 100.000 0.458 2 MULITE DOUBLT MULITE DOUBLT 100.000 0.411 3 MULITE DOUBLT MULITE DOUBLT 100.000 0.414 MULITE DOUBLT Wt Mean 100.000 0.246 0.000 3 File analyte line Irel=100 line relative Standard Root mean Number of # Phase h k l Name h k l Intensity Deviation square dev. measurments 1 MULITE 2 1 0 MULITE DOUBLT 56.373 0.195 2 MULITE 2 1 0 MULITE DOUBLT 59.030 0.183 3 MULITE 2 1 0 MULITE DOUBLT 55.423 0.174 MULITE 2 1 0 Wt Mean 56.909 0.106 1.097 3 File analyte line Irel=100 line relative Standard Root mean Number of # Phase h k l Name h k l Intensity Deviation square dev. measurments 1 MULITE 2 2 0 MULITE DOUBLT 32.172 0.211 2 MULITE 2 2 0 MULITE DOUBLT 24.742 0.171 3 MULITE 2 2 0 MULITE DOUBLT 32.642 0.191 MULITE 2 2 0 Wt Mean 29.302 0.109 2.674 3 File analyte line Irel=100 line relative Standard Root mean Number of # Phase h k l Name h k l Intensity Deviation square dev. measurments 1 MULITE 1 1 1 MULITE DOUBLT 36.828 0.262 2 MULITE 1 1 1 MULITE DOUBLT 33.369 0.224 3 MULITE 1 1 1 MULITE DOUBLT 36.135 0.235 MULITE 1 1 1 Wt Mean 35.282 0.138 1.071 3 File analyte line Irel=100 line relative Standard Root mean Number of # Phase h k l Name h k l Intensity Deviation square dev. measurments 1 MULITE 1 2 1 MULITE DOUBLT 42.818 0.313 2 MULITE 1 2 1 MULITE DOUBLT 39.234 0.268 3 MULITE 1 2 1 MULITE DOUBLT 42.741 0.282 MULITE 1 2 1 Wt Mean 41.429 0.165 1.216 3 File analyte line Irel=100 line relative Standard Root mean Number of # Phase h k l Name h k l Intensity Deviation square dev. measurments 1 MULITE 3 2 0 MULITE DOUBLT 18.282 0.221 2 MULITE 3 2 0 MULITE DOUBLT 15.736 0.190 3 MULITE 3 2 0 MULITE DOUBLT 17.075 0.195 MULITE 3 2 0 Wt Mean 16.909 0.116 0.722 3 File analyte line Irel=100 line relative Standard Root mean Number of # Phase h k l Name h k l Intensity Deviation square dev. measurments 1 SILICN 1 1 1 SILICN 1 1 1 100.000 0.183 2 SILICN 1 1 1 SILICN 1 1 1 100.000 0.178 3 SILICN 1 1 1 SILICN 1 1 1 100.000 0.174 SILICN 1 1 1 Wt Mean 100.000 0.103 0.000 3 File analyte line Irel=100 line relative Standard Root mean Number of # Phase h k l Name h k l Intensity Deviation square dev. measurments 1 SILICN 3 1 1 SILICN 1 1 1 32.482 0.130 2 SILICN 3 1 1 SILICN 1 1 1 31.908 0.125 3 SILICN 3 1 1 SILICN 1 1 1 30.495 0.120 SILICN 3 1 1 Wt Mean 31.575 0.072 0.596 3 File analyte line Irel=100 line relative Standard Root mean Number of # Phase h k l Name h k l Intensity Deviation square dev. measurments 1 SILICN 3 1 1 SILICN 1 1 1 22.506 0.058 2 SILICN 3 1 1 SILICN 1 1 1 22.835 0.057 3 SILICN 3 1 1 SILICN 1 1 1 22.825 0.056 SILICN 3 1 1 Wt Mean 22.727 0.033 0.107 3 Summary of relative intensities Phase h k l Method Intensity e.s.d. rms dev # MULITE 1 1 0 INTEGRT 43.012 0.094 0.814 3 MULITE DOUBLT INTEGRT 100.000 0.246 0.000 3 MULITE 2 1 0 PEAK HT 56.909 0.106 1.097 3 MULITE 2 2 0 INTEGRT 29.302 0.109 2.674 3 MULITE 1 1 1 INTEGRT 35.282 0.138 1.071 3 MULITE 1 2 1 INTEGRT 41.429 0.165 1.216 3 MULITE 3 2 0 INTEGRT 16.909 0.116 0.722 3 Phase h k l Method Intensity e.s.d. rms dev # SILICN 1 1 1 INTEGRT 100.000 0.103 0.000 3 SILICN 3 1 1 INTEGRT 31.575 0.072 0.596 3 SILICN 3 1 1 PEAK HT 22.727 0.033 0.107 3 RIR Calibration for quantitative analysis by the internal standard method ***** Line by line RIR analysis ***** File Analyte Line Standard Line RIR Standard Root Mean Number of Degrees of # Phase h k l Name h k l Constant Deviation square dev. measurments freedom 1 MULITE 1 1 0 SILICN 1 1 1 0.2361 0.0009 2 MULITE 1 1 0 SILICN 1 1 1 0.2527 0.0009 3 MULITE 1 1 0 SILICN 1 1 1 0.2541 0.0009 MULITE 1 1 0 Wt Mean 1 1 1 0.2474 0.0005 0.0058 3 2 File Analyte Line Standard Line RIR Standard Root Mean Number of Degrees of # Phase h k l Name h k l Constant Deviation square dev. measurments freedom 1 MULITE DOUBLT SILICN 1 1 1 0.2338 0.0010 2 MULITE DOUBLT SILICN 1 1 1 0.2614 0.0011 3 MULITE DOUBLT SILICN 1 1 1 0.2471 0.0010 MULITE DOUBLT Wt Mean 1 1 1 0.2469 0.0006 0.0079 3 2 File Analyte Line Standard Line RIR Standard Root Mean Number of Degrees of # Phase h k l Name h k l Constant Deviation square dev. measurments freedom 1 MULITE 2 1 0 SILICN 1 1 1 0.2316 0.0006 2 MULITE 2 1 0 SILICN 1 1 1 0.2711 0.0007 3 MULITE 2 1 0 SILICN 1 1 1 0.2406 0.0007 MULITE 2 1 0 Wt Mean 1 1 1 0.2459 0.0004 0.0115 3 2 File Analyte Line Standard Line RIR Standard Root Mean Number of Degrees of # Phase h k l Name h k l Constant Deviation square dev. measurments freedom 1 MULITE 2 2 0 SILICN 1 1 1 0.2567 0.0018 2 MULITE 2 2 0 SILICN 1 1 1 0.2207 0.0016 3 MULITE 2 2 0 SILICN 1 1 1 0.2752 0.0018 MULITE 2 2 0 Wt Mean 1 1 1 0.2492 0.0010 0.0163 3 2 File Analyte Line Standard Line RIR Standard Root Mean Number of Degrees of # Phase h k l Name h k l Constant Deviation square dev. measurments freedom 1 MULITE 1 1 1 SILICN 1 1 1 0.2440 0.0019 2 MULITE 1 1 1 SILICN 1 1 1 0.2472 0.0018 3 MULITE 1 1 1 SILICN 1 1 1 0.2530 0.0018 MULITE 1 1 1 Wt Mean 1 1 1 0.2482 0.0011 0.0026 3 2 File Analyte Line Standard Line RIR Standard Root Mean Number of Degrees of # Phase h k l Name h k l Constant Deviation square dev. measurments freedom 1 MULITE 1 2 1 SILICN 1 1 1 0.2416 0.0019 2 MULITE 1 2 1 SILICN 1 1 1 0.2476 0.0019 3 MULITE 1 2 1 SILICN 1 1 1 0.2549 0.0019 MULITE 1 2 1 Wt Mean 1 1 1 0.2481 0.0011 0.0038 3 2 File Analyte Line Standard Line RIR Standard Root Mean Number of Degrees of # Phase h k l Name h k l Constant Deviation square dev. measurments freedom 1 MULITE 3 2 0 SILICN 1 1 1 0.2528 0.0034 2 MULITE 3 2 0 SILICN 1 1 1 0.2433 0.0033 3 MULITE 3 2 0 SILICN 1 1 1 0.2495 0.0033 MULITE 3 2 0 Wt Mean 1 1 1 0.2484 0.0019 0.0028 3 2 File Analyte Line Standard Line RIR Standard Root Mean Number of Degrees of # Phase h k l Name h k l Constant Deviation square dev. measurments freedom 1 MULITE 1 1 0 SILICN 3 1 1 0.2295 0.0013 2 MULITE 1 1 0 SILICN 3 1 1 0.2501 0.0013 3 MULITE 1 1 0 SILICN 3 1 1 0.2631 0.0014 MULITE 1 1 0 Wt Mean 3 1 1 0.2463 0.0008 0.0098 3 2 File Analyte Line Standard Line RIR Standard Root Mean Number of Degrees of # Phase h k l Name h k l Constant Deviation square dev. measurments freedom 1 MULITE DOUBLT SILICN 3 1 1 0.2273 0.0014 2 MULITE DOUBLT SILICN 3 1 1 0.2587 0.0015 3 MULITE DOUBLT SILICN 3 1 1 0.2558 0.0015 MULITE DOUBLT Wt Mean 3 1 1 0.2460 0.0008 0.0103 3 2 File Analyte Line Standard Line RIR Standard Root Mean Number of Degrees of # Phase h k l Name h k l Constant Deviation square dev. measurments freedom 1 MULITE 2 1 0 SILICN 3 1 1 0.2251 0.0011 2 MULITE 2 1 0 SILICN 3 1 1 0.2683 0.0013 3 MULITE 2 1 0 SILICN 3 1 1 0.2491 0.0012 MULITE 2 1 0 Wt Mean 3 1 1 0.2453 0.0007 0.0125 3 2 File Analyte Line Standard Line RIR Standard Root Mean Number of Degrees of # Phase h k l Name h k l Constant Deviation square dev. measurments freedom 1 MULITE 2 2 0 SILICN 3 1 1 0.2495 0.0020 2 MULITE 2 2 0 SILICN 3 1 1 0.2184 0.0019 3 MULITE 2 2 0 SILICN 3 1 1 0.2850 0.0022 MULITE 2 2 0 Wt Mean 3 1 1 0.2474 0.0012 0.0191 3 2 File Analyte Line Standard Line RIR Standard Root Mean Number of Degrees of # Phase h k l Name h k l Constant Deviation square dev. measurments freedom 1 MULITE 1 1 1 SILICN 3 1 1 0.2372 0.0021 2 MULITE 1 1 1 SILICN 3 1 1 0.2447 0.0021 3 MULITE 1 1 1 SILICN 3 1 1 0.2620 0.0022 MULITE 1 1 1 Wt Mean 3 1 1 0.2475 0.0012 0.0072 3 2 File Analyte Line Standard Line RIR Standard Root Mean Number of Degrees of # Phase h k l Name h k l Constant Deviation square dev. measurments freedom 1 MULITE 1 2 1 SILICN 3 1 1 0.2349 0.0021 2 MULITE 1 2 1 SILICN 3 1 1 0.2450 0.0021 3 MULITE 1 2 1 SILICN 3 1 1 0.2639 0.0022 MULITE 1 2 1 Wt Mean 3 1 1 0.2473 0.0012 0.0084 3 2 File Analyte Line Standard Line RIR Standard Root Mean Number of Degrees of # Phase h k l Name h k l Constant Deviation square dev. measurments freedom 1 MULITE 3 2 0 SILICN 3 1 1 0.2457 0.0035 2 MULITE 3 2 0 SILICN 3 1 1 0.2407 0.0034 3 MULITE 3 2 0 SILICN 3 1 1 0.2583 0.0035 MULITE 3 2 0 Wt Mean 3 1 1 0.2481 0.0020 0.0052 3 2 File Analyte Line Standard Line RIR Standard Root Mean Number of Degrees of # Phase h k l Name h k l Constant Deviation square dev. measurments freedom 1 MULITE 1 1 0 SILICN 3 1 1 0.2384 0.0010 2 MULITE 1 1 0 SILICN 3 1 1 0.2515 0.0010 3 MULITE 1 1 0 SILICN 3 1 1 0.2530 0.0010 MULITE 1 1 0 Wt Mean 3 1 1 0.2476 0.0006 0.0047 3 2 File Analyte Line Standard Line RIR Standard Root Mean Number of Degrees of # Phase h k l Name h k l Constant Deviation square dev. measurments freedom 1 MULITE DOUBLT SILICN 3 1 1 0.2361 0.0011 2 MULITE DOUBLT SILICN 3 1 1 0.2602 0.0012 3 MULITE DOUBLT SILICN 3 1 1 0.2460 0.0011 MULITE DOUBLT Wt Mean 3 1 1 0.2470 0.0007 0.0069 3 2 File Analyte Line Standard Line RIR Standard Root Mean Number of Degrees of # Phase h k l Name h k l Constant Deviation square dev. measurments freedom 1 MULITE 2 1 0 SILICN 3 1 1 0.2339 0.0008 2 MULITE 2 1 0 SILICN 3 1 1 0.2699 0.0009 3 MULITE 2 1 0 SILICN 3 1 1 0.2396 0.0008 MULITE 2 1 0 Wt Mean 3 1 1 0.2461 0.0005 0.0107 3 2 File Analyte Line Standard Line RIR Standard Root Mean Number of Degrees of # Phase h k l Name h k l Constant Deviation square dev. measurments freedom 1 MULITE 2 2 0 SILICN 3 1 1 0.2592 0.0019 2 MULITE 2 2 0 SILICN 3 1 1 0.2197 0.0017 3 MULITE 2 2 0 SILICN 3 1 1 0.2740 0.0019 MULITE 2 2 0 Wt Mean 3 1 1 0.2489 0.0010 0.0167 3 2 File Analyte Line Standard Line RIR Standard Root Mean Number of Degrees of # Phase h k l Name h k l Constant Deviation square dev. measurments freedom 1 MULITE 1 1 1 SILICN 3 1 1 0.2464 0.0019 2 MULITE 1 1 1 SILICN 3 1 1 0.2461 0.0019 3 MULITE 1 1 1 SILICN 3 1 1 0.2519 0.0019 MULITE 1 1 1 Wt Mean 3 1 1 0.2482 0.0011 0.0019 3 2 File Analyte Line Standard Line RIR Standard Root Mean Number of Degrees of # Phase h k l Name h k l Constant Deviation square dev. measurments freedom 1 MULITE 1 2 1 SILICN 3 1 1 0.2440 0.0020 2 MULITE 1 2 1 SILICN 3 1 1 0.2464 0.0019 3 MULITE 1 2 1 SILICN 3 1 1 0.2538 0.0019 MULITE 1 2 1 Wt Mean 3 1 1 0.2481 0.0011 0.0029 3 2 File Analyte Line Standard Line RIR Standard Root Mean Number of Degrees of # Phase h k l Name h k l Constant Deviation square dev. measurments freedom 1 MULITE 3 2 0 SILICN 3 1 1 0.2553 0.0035 2 MULITE 3 2 0 SILICN 3 1 1 0.2421 0.0033 3 MULITE 3 2 0 SILICN 3 1 1 0.2484 0.0033 MULITE 3 2 0 Wt Mean 3 1 1 0.2484 0.0020 0.0037 3 2 Wt Mean Over the standard lines used: File Analyte Line Standard Line RIR Standard Root Mean Number of Degrees of # Phase h k l Name h k l Constant Deviation square dev. measurments freedom MULITE 1 1 0 SILICN all 0.2472 0.0003 0.0041 9 5 MULITE DOUBLT SILICN all 0.2468 0.0004 0.0047 9 6 MULITE 2 1 0 SILICN all 0.2459 0.0003 0.0072 9 5 MULITE 2 2 0 SILICN all 0.2486 0.0006 0.0109 9 5 MULITE 1 1 1 SILICN all 0.2480 0.0006 0.0027 9 5 MULITE 1 2 1 SILICN all 0.2479 0.0007 0.0034 9 5 MULITE 3 2 0 SILICN all 0.2483 0.0011 0.0025 9 5 Overall Wt Mean over all lines for each phase: File Analyte Line Standard Line RIR Standard Root Mean Number of Degrees of # Phase h k l Name h k l Constant Deviation square dev. measurments freedom MULITE all SILICN all 0.2469 0.0002 0.0023 63 36 Are files for another calibration phase to be entered? (y/n) Y Input all the files for calibration phase number 3 Enter a blank for the requested file name after the last file for this phase has been processed Enter name for file # 1 CR063D Title: HEMATITE-SI BINARY TEST OF INTERNAL STANDARD METHOD JOHN J. SIMMINS Enter name for file # 2 CR066D Title: 60%HEMATITE; 40%SI; SPRAY DRIED; JOHN J. SIMMINS Enter name for file # 5 Relative intensity analysis: The following line(s) will be used in scaling ln Phase h k l Method 3 HEMATI 1 0 4 INTEGRT 2 SILICN 1 1 1 INTEGRT File analyte line Irel=100 line relative Standard Root mean Number of # Phase h k l Name h k l Intensity Deviation square dev. measurments 1 HEMATI 0 1 2 HEMATI 1 0 4 26.540 0.151 2 HEMATI 0 1 2 HEMATI 1 0 4 28.862 0.150 3 HEMATI 0 1 2 HEMATI 1 0 4 27.640 0.144 4 HEMATI 0 1 2 HEMATI 1 0 4 28.239 0.148 HEMATI 0 1 2 Wt Mean 27.824 0.074 0.488 4 File analyte line Irel=100 line relative Standard Root mean Number of # Phase h k l Name h k l Intensity Deviation square dev. measurments 1 HEMATI 1 0 4 HEMATI 1 0 4 100.000 0.449 2 HEMATI 1 0 4 HEMATI 1 0 4 100.000 0.438 3 HEMATI 1 0 4 HEMATI 1 0 4 100.000 0.429 4 HEMATI 1 0 4 HEMATI 1 0 4 100.000 0.436 HEMATI 1 0 4 Wt Mean 100.000 0.219 0.000 4 File analyte line Irel=100 line relative Standard Root mean Number of # Phase h k l Name h k l Intensity Deviation square dev. measurments 1 HEMATI 1 1 0 HEMATI 1 0 4 65.898 0.332 2 HEMATI 1 1 0 HEMATI 1 0 4 66.265 0.326 3 HEMATI 1 1 0 HEMATI 1 0 4 65.854 0.319 4 HEMATI 1 1 0 HEMATI 1 0 4 64.974 0.320 HEMATI 1 1 0 Wt Mean 65.740 0.162 0.276 4 File analyte line Irel=100 line relative Standard Root mean Number of # Phase h k l Name h k l Intensity Deviation square dev. measurments 1 HEMATI 1 1 3 HEMATI 1 0 4 21.754 0.215 2 HEMATI 1 1 3 HEMATI 1 0 4 22.649 0.210 3 HEMATI 1 1 3 HEMATI 1 0 4 22.417 0.206 4 HEMATI 1 1 3 HEMATI 1 0 4 21.770 0.206 HEMATI 1 1 3 Wt Mean 22.150 0.105 0.227 4 File analyte line Irel=100 line relative Standard Root mean Number of # Phase h k l Name h k l Intensity Deviation square dev. measurments 1 HEMATI 2 1 4 HEMATI 1 0 4 26.653 0.255 2 HEMATI 2 1 4 HEMATI 1 0 4 28.364 0.259 3 HEMATI 2 1 4 HEMATI 1 0 4 27.675 0.256 4 HEMATI 2 1 4 HEMATI 1 0 4 27.864 0.254 HEMATI 2 1 4 Wt Mean 27.635 0.128 0.359 4 File analyte line Irel=100 line relative Standard Root mean Number of # Phase h k l Name h k l Intensity Deviation square dev. measurments 1 SILICN 1 1 1 SILICN 1 1 1 100.000 0.362 2 SILICN 1 1 1 SILICN 1 1 1 100.000 0.346 3 SILICN 1 1 1 SILICN 1 1 1 100.000 0.342 4 SILICN 1 1 1 SILICN 1 1 1 100.000 0.336 SILICN 1 1 1 Wt Mean 100.000 0.173 0.000 4 File analyte line Irel=100 line relative Standard Root mean Number of # Phase h k l Name h k l Intensity Deviation square dev. measurments 1 SILICN 3 1 1 SILICN 1 1 1 33.548 0.250 2 SILICN 3 1 1 SILICN 1 1 1 33.636 0.244 3 SILICN 3 1 1 SILICN 1 1 1 34.534 0.244 4 SILICN 3 1 1 SILICN 1 1 1 32.846 0.233 SILICN 3 1 1 Wt Mean 33.623 0.121 0.351 4 File analyte line Irel=100 line relative Standard Root mean Number of # Phase h k l Name h k l Intensity Deviation square dev. measurments 1 SILICN 3 1 1 SILICN 1 1 1 26.936 0.100 2 SILICN 3 1 1 SILICN 1 1 1 27.024 0.096 3 SILICN 3 1 1 SILICN 1 1 1 27.126 0.095 4 SILICN 3 1 1 SILICN 1 1 1 25.355 0.089 SILICN 3 1 1 Wt Mean 26.559 0.047 0.437 4 Summary of relative intensities Phase h k l Method Intensity e.s.d. rms dev # HEMATI 0 1 2 INTEGRT 27.824 0.074 0.488 4 HEMATI 1 0 4 INTEGRT 100.000 0.219 0.000 4 HEMATI 1 1 0 INTEGRT 65.740 0.162 0.276 4 HEMATI 1 1 3 INTEGRT 22.150 0.105 0.227 4 HEMATI 2 1 4 INTEGRT 27.635 0.128 0.359 4 Phase h k l Method Intensity e.s.d. rms dev # SILICN 1 1 1 INTEGRT 100.000 0.173 0.000 4 SILICN 3 1 1 INTEGRT 33.623 0.121 0.351 4 SILICN 3 1 1 PEAK HT 26.559 0.047 0.437 4 RIR Calibration for quantitative analysis by the internal standard method ***** Line by line RIR analysis ***** File Analyte Line Standard Line RIR Standard Root Mean Number of Degrees of # Phase h k l Name h k l Constant Deviation square dev. measurments freedom 1 HEMATI 0 1 2 SILICN 1 1 1 0.6298 0.0039 2 HEMATI 0 1 2 SILICN 1 1 1 0.6817 0.0039 3 HEMATI 0 1 2 SILICN 1 1 1 0.6555 0.0038 4 HEMATI 0 1 2 SILICN 1 1 1 0.6475 0.0037 HEMATI 0 1 2 Wt Mean 1 1 1 0.6534 0.0019 0.0106 4 3 File Analyte Line Standard Line RIR Standard Root Mean Number of Degrees of # Phase h k l Name h k l Constant Deviation square dev. measurments freedom 1 HEMATI 1 0 4 SILICN 1 1 1 0.6603 0.0033 2 HEMATI 1 0 4 SILICN 1 1 1 0.6572 0.0032 3 HEMATI 1 0 4 SILICN 1 1 1 0.6599 0.0032 4 HEMATI 1 0 4 SILICN 1 1 1 0.6380 0.0031 HEMATI 1 0 4 Wt Mean 1 1 1 0.6534 0.0016 0.0054 4 3 File Analyte Line Standard Line RIR Standard Root Mean Number of Degrees of # Phase h k l Name h k l Constant Deviation square dev. measurments freedom 1 HEMATI 1 1 0 SILICN 1 1 1 0.6618 0.0037 2 HEMATI 1 1 0 SILICN 1 1 1 0.6624 0.0036 3 HEMATI 1 1 0 SILICN 1 1 1 0.6610 0.0036 4 HEMATI 1 1 0 SILICN 1 1 1 0.6305 0.0034 HEMATI 1 1 0 Wt Mean 1 1 1 0.6533 0.0018 0.0080 4 3 File Analyte Line Standard Line RIR Standard Root Mean Number of Degrees of # Phase h k l Name h k l Constant Deviation square dev. measurments freedom 1 HEMATI 1 1 3 SILICN 1 1 1 0.6484 0.0071 2 HEMATI 1 1 3 SILICN 1 1 1 0.6720 0.0070 3 HEMATI 1 1 3 SILICN 1 1 1 0.6678 0.0069 4 HEMATI 1 1 3 SILICN 1 1 1 0.6270 0.0066 HEMATI 1 1 3 Wt Mean 1 1 1 0.6532 0.0034 0.0105 4 3 File Analyte Line Standard Line RIR Standard Root Mean Number of Degrees of # Phase h k l Name h k l Constant Deviation square dev. measurments freedom 1 HEMATI 2 1 4 SILICN 1 1 1 0.6368 0.0068 2 HEMATI 2 1 4 SILICN 1 1 1 0.6745 0.0069 3 HEMATI 2 1 4 SILICN 1 1 1 0.6608 0.0068 4 HEMATI 2 1 4 SILICN 1 1 1 0.6432 0.0065 HEMATI 2 1 4 Wt Mean 1 1 1 0.6535 0.0034 0.0085 4 3 File Analyte Line Standard Line RIR Standard Root Mean Number of Degrees of # Phase h k l Name h k l Constant Deviation square dev. measurments freedom 1 HEMATI 0 1 2 SILICN 3 1 1 0.6312 0.0060 2 HEMATI 0 1 2 SILICN 3 1 1 0.6814 0.0063 3 HEMATI 0 1 2 SILICN 3 1 1 0.6382 0.0058 4 HEMATI 0 1 2 SILICN 3 1 1 0.6628 0.0060 HEMATI 0 1 2 Wt Mean 3 1 1 0.6526 0.0030 0.0114 4 3 File Analyte Line Standard Line RIR Standard Root Mean Number of Degrees of # Phase h k l Name h k l Constant Deviation square dev. measurments freedom 1 HEMATI 1 0 4 SILICN 3 1 1 0.6617 0.0058 2 HEMATI 1 0 4 SILICN 3 1 1 0.6569 0.0057 3 HEMATI 1 0 4 SILICN 3 1 1 0.6425 0.0054 4 HEMATI 1 0 4 SILICN 3 1 1 0.6530 0.0055 HEMATI 1 0 4 Wt Mean 3 1 1 0.6532 0.0028 0.0041 4 3 File Analyte Line Standard Line RIR Standard Root Mean Number of Degrees of # Phase h k l Name h k l Constant Deviation square dev. measurments freedom 1 HEMATI 1 1 0 SILICN 3 1 1 0.6633 0.0061 2 HEMATI 1 1 0 SILICN 3 1 1 0.6622 0.0059 3 HEMATI 1 1 0 SILICN 3 1 1 0.6436 0.0057 4 HEMATI 1 1 0 SILICN 3 1 1 0.6454 0.0057 HEMATI 1 1 0 Wt Mean 3 1 1 0.6531 0.0029 0.0053 4 3 File Analyte Line Standard Line RIR Standard Root Mean Number of Degrees of # Phase h k l Name h k l Constant Deviation square dev. measurments freedom 1 HEMATI 1 1 3 SILICN 3 1 1 0.6499 0.0085 2 HEMATI 1 1 3 SILICN 3 1 1 0.6717 0.0085 3 HEMATI 1 1 3 SILICN 3 1 1 0.6502 0.0081 4 HEMATI 1 1 3 SILICN 3 1 1 0.6418 0.0081 HEMATI 1 1 3 Wt Mean 3 1 1 0.6531 0.0041 0.0063 4 3 File Analyte Line Standard Line RIR Standard Root Mean Number of Degrees of # Phase h k l Name h k l Constant Deviation square dev. measurments freedom 1 HEMATI 2 1 4 SILICN 3 1 1 0.6382 0.0082 2 HEMATI 2 1 4 SILICN 3 1 1 0.6743 0.0084 3 HEMATI 2 1 4 SILICN 3 1 1 0.6434 0.0080 4 HEMATI 2 1 4 SILICN 3 1 1 0.6585 0.0081 HEMATI 2 1 4 Wt Mean 3 1 1 0.6533 0.0041 0.0080 4 3 File Analyte Line Standard Line RIR Standard Root Mean Number of Degrees of # Phase h k l Name h k l Constant Deviation square dev. measurments freedom 1 HEMATI 0 1 2 SILICN 3 1 1 0.6210 0.0039 2 HEMATI 0 1 2 SILICN 3 1 1 0.6700 0.0039 3 HEMATI 0 1 2 SILICN 3 1 1 0.6418 0.0038 4 HEMATI 0 1 2 SILICN 3 1 1 0.6782 0.0040 HEMATI 0 1 2 Wt Mean 3 1 1 0.6522 0.0020 0.0131 4 3 File Analyte Line Standard Line RIR Standard Root Mean Number of Degrees of # Phase h k l Name h k l Constant Deviation square dev. measurments freedom 1 HEMATI 1 0 4 SILICN 3 1 1 0.6510 0.0033 2 HEMATI 1 0 4 SILICN 3 1 1 0.6459 0.0032 3 HEMATI 1 0 4 SILICN 3 1 1 0.6461 0.0031 4 HEMATI 1 0 4 SILICN 3 1 1 0.6682 0.0033 HEMATI 1 0 4 Wt Mean 3 1 1 0.6525 0.0016 0.0052 4 3 File Analyte Line Standard Line RIR Standard Root Mean Number of Degrees of # Phase h k l Name h k l Constant Deviation square dev. measurments freedom 1 HEMATI 1 1 0 SILICN 3 1 1 0.6526 0.0037 2 HEMATI 1 1 0 SILICN 3 1 1 0.6510 0.0036 3 HEMATI 1 1 0 SILICN 3 1 1 0.6472 0.0036 4 HEMATI 1 1 0 SILICN 3 1 1 0.6604 0.0037 HEMATI 1 1 0 Wt Mean 3 1 1 0.6527 0.0018 0.0028 4 3 File Analyte Line Standard Line RIR Standard Root Mean Number of Degrees of # Phase h k l Name h k l Constant Deviation square dev. measurments freedom 1 HEMATI 1 1 3 SILICN 3 1 1 0.6394 0.0070 2 HEMATI 1 1 3 SILICN 3 1 1 0.6604 0.0069 3 HEMATI 1 1 3 SILICN 3 1 1 0.6539 0.0068 4 HEMATI 1 1 3 SILICN 3 1 1 0.6568 0.0070 HEMATI 1 1 3 Wt Mean 3 1 1 0.6527 0.0035 0.0046 4 3 File Analyte Line Standard Line RIR Standard Root Mean Number of Degrees of # Phase h k l Name h k l Constant Deviation square dev. measurments freedom 1 HEMATI 2 1 4 SILICN 3 1 1 0.6279 0.0067 2 HEMATI 2 1 4 SILICN 3 1 1 0.6629 0.0068 3 HEMATI 2 1 4 SILICN 3 1 1 0.6470 0.0067 4 HEMATI 2 1 4 SILICN 3 1 1 0.6738 0.0069 HEMATI 2 1 4 Wt Mean 3 1 1 0.6525 0.0034 0.0100 4 3 Wt Mean Over the standard lines used: File Analyte Line Standard Line RIR Standard Root Mean Number of Degrees of # Phase h k l Name h k l Constant Deviation square dev. measurments freedom HEMATI 0 1 2 SILICN all 0.6528 0.0012 0.0072 12 8 HEMATI 1 0 4 SILICN all 0.6530 0.0010 0.0030 12 9 HEMATI 1 1 0 SILICN all 0.6530 0.0012 0.0036 12 8 HEMATI 1 1 3 SILICN all 0.6530 0.0021 0.0047 12 8 HEMATI 2 1 4 SILICN all 0.6531 0.0021 0.0055 12 8 Overall Wt Mean over all lines for each phase: File Analyte Line Standard Line RIR Standard Root Mean Number of Degrees of # Phase h k l Name h k l Constant Deviation square dev. measurments freedom HEMATI all SILICN all 0.6530 0.0006 0.0021 60 41 Are files for another calibration phase to be entered? (y/n) N Enter the name of the RUN file If an extension is not typed .RUN will be appended CR072R Enter the title for the RUN file INTERNAL STANDARD RUN FILE FOR HEMATITE+HEMATITE+QUARTZ WITH A SI STD. Enter your name CAMDEN HUBBARD Enter the maximum time, in minutes, to be spent counting each peak 5.0 Enter the percent error to which each peak should be counted (eg. 0.5%) If zero each peak will be counted for a fixed time of 5.00 minutes 1.0 Listing of the output RUN file:CR072R.RUN INTERNAL STANDARD RUN FILE FOR HEMATITE+HEMATITE+QUARTZ WITH A SI STD. 15.650 16.430 17.000 0.010030.00 5.0 1.00 32700.MULITE 1 1 0100 910 43.010.09 0.2469 0.0002 0.000 0.00 0.0000 0.00 0.00 0.00 0.00 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 20.400 20.850 21.200 0.010030.00 5.0 1.00 32700.QUARTZ 1 0 0100 910 17.650.02 0.9277 0.0004 0.000 0.00 0.0000 0.00 0.00 0.00 0.00 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 23.700 24.140 25.000 0.010030.00 5.0 1.00 32700.HEMATI 0 1 2100 910 27.820.07 0.6530 0.0006 0.000 0.00 0.0000 0.00 0.00 0.00 0.00 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 The line MULITE 2 1 0 26.220 is pk height mode and The line MULITEDOUBLT 26.270 is integrate mode Do you wish to collect peak height as well as integrated data? (Y/N) N The following two lines are within 1 degree of each other MULITEDOUBLT 26.270 IPK=0 QUARTZ 1 0 1 26.650 IPK=0 Should they be treated as overlapping? (y/n) Y Overlap condition being set for reflections: MULITEDOUBLT QUARTZ 1 0 1 The line QUARTZ 1 0 1 26.650 is specified integrate mode and The line QUARTZ 1 0 1 26.680 is specified peak height mode Do you wish to collect peak height as well as integrated data (yes/no)? N 25.000 26.650 27.550 0.010030.00 5.0 1.00 32700.QUARTZ 1 0 1110 910100.000.08 0.9277 0.0004 0.000 0.00 0.0000 MULITEDOUBLT100.00 0.25 0.00 0.00 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 27.500 28.440 29.400 0.010030.00 5.0 1.00 32700.SILICN 1 1 1200 910100.000.06 -0.5000 -0.5000 0.000 0.00 0.0000 0.00 0.00 0.00 0.00 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 The following two lines are within 1 degree of each other HEMATI 1 0 4 33.150 IPK=0 MULITE 2 2 0 33.230 IPK=0 Should they be treated as overlapping? (y/n) Y Overlap condition being set for reflections: HEMATI 1 0 4 MULITE 2 2 0 32.100 33.230 34.200 0.010030.00 5.0 1.00 32700.MULITE 2 2 0110 910 29.300.11 0.2469 0.0002 0.000 0.00 0.0000 HEMATI 1 0 4100.00 0.22 0.00 0.00 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 The following two lines are within 1 degree of each other MULITE 1 1 1 35.280 IPK=0 HEMATI 1 1 0 35.610 IPK=0 Should they be treated as overlapping? (y/n) Y Overlap condition being set for reflections: MULITE 1 1 1 HEMATI 1 1 0 34.350 35.610 36.200 0.010030.00 5.0 1.00 32700.HEMATI 1 1 0110 910 65.740.16 0.6530 0.0006 0.000 0.00 0.0000 MULITE 1 1 1 35.28 0.14 0.00 0.00 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 The following two lines are within 1 degree of each other QUARTZ 1 1 1 40.290 IPK=0 HEMATI 1 1 3 40.860 IPK=0 Should they be treated as overlapping? (y/n) Y Overlap condition being set for reflections: QUARTZ 1 1 1 HEMATI 1 1 3 Overlap condition being set for reflections: HEMATI 1 1 3 MULITE 1 2 1 39.800 40.860 41.750 0.010030.00 5.0 1.00 32700.HEMATI 1 1 3120 910 22.150.10 0.6530 0.0006 0.000 0.00 0.0000 QUARTZ 1 1 1 3.01 0.03MULITE 1 2 1 41.43 0.17 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 Overlap condition being set for reflections: QUARTZ 2 0 0 MULITE 3 2 0 41.750 42.920 43.300 0.010030.00 5.0 1.00 32700.MULITE 3 2 0110 910 16.910.12 0.2469 0.0002 0.000 0.00 0.0000 QUARTZ 2 0 0 4.83 0.02 0.00 0.00 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 The line SILICN 3 1 1 56.123 is specified integrate mode and The line SILICN 3 1 1 56.133 is specified peak height mode Do you wish to collect peak height as well as integrated data (yes/no)? N 55.550 56.123 56.850 0.010030.00 5.0 1.00 32700.SILICN 3 1 1200 910 31.430.04 -0.5000 -0.5000 0.000 0.00 0.0000 0.00 0.00 0.00 0.00 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 61.700 62.450 63.000 0.010030.00 5.0 1.00 32700.HEMATI 2 1 4100 910 27.630.13 0.6530 0.0006 0.000 0.00 0.0000 0.00 0.00 0.00 0.00 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 11 Lines output to the runfile with 2 unoverlapped standard lines $