$ RUN AMORPHOUS NBS*QUANT84-AMORPHOUS Revision Date: 29 feb1984 Amorphous quantitative analysis by the spiking method Written by C. R. Hubbard Run on 5-AUG-8 at 01:10:09 Select Output Mode Desired: (Output is 132 characters wide) 1 - causes output to be put on the interactive terminal. newname - causes output to go to the named file. - causes output to go to a file named AMORPHOUS.LIS. Enter the output destination: 1 Select a print control option (I1): 0 = Full listing of data files 1 = Heading on first data file only 2 = Data file titles only 2 Enter weighting choice: 0 for counting statistical weights 1 for unit weights 0 Enter Orig. Sample file name CH291D Title: ZERO SPIKE OF B#115 WITH NEW AMORPH. RANGES JOHN J. SIMMINS Enter Orig.+ Spike file name CH292D Title: APPROX.0.05GM ZEOTHIX/GM QTZ.B/3115; NEW AM. REGIONS JOHN J. SIMMINS Enter Orig.+ Spike file name CH293D Title: APPROX.0.1 GM ZEOTHIX/GM QTZ.B#115; NEW AM. REGIONS JOHN J. SIMMINS Enter Orig.+ Spike file name CH294D Title: APPROX. 0.15GM ZEOTHIX/0.5GM QTZ.B#115; NEW AM. REGIONS JOHN J. SIMMINS Enter Orig.+ Spike file name Enter Background file name CH295D Title: 400 MESH QTZ BACKGROUND WITH NEW AMORPHOUS REGIONS JOHN J. SIMMINS Line by line composition analysis from Weighted linear regressions of 4 points per analysis Analyte Line Reference Line Weight Least Sqs Phase h k l Name h k l Percent Est Std Dev Slope Intercept correlation AMORPH AREA 1 QUARTZ 1 0 0 5.21 0.77 0.9146(0.0437) 0.0476(0.0066) 1.014 gms added Obs esd Calc Delta per gm Ia/Ir Ia/Ir Ia/Ir Ia/Ir 0.0000 0.0456 0.0009 0.0476 0.0021 0.1001 0.1394 0.0010 0.1392 -0.0002 0.1990 0.2410 0.0012 0.2297 -0.0113 0.3004 0.3117 0.0014 0.3224 0.0107 AMORPH AREA 2 QUARTZ 1 0 0 4.15 0.19 1.6665(0.0227) 0.0692(0.0030) 1.008 gms added Obs esd Calc Delta per gm Ia/Ir Ia/Ir Ia/Ir Ia/Ir 0.0000 0.0684 0.0009 0.0692 0.0009 0.1001 0.2367 0.0011 0.2361 -0.0007 0.1990 0.4065 0.0015 0.4009 -0.0056 0.3004 0.5626 0.0020 0.5698 0.0072 AMORPH AREA 3 QUARTZ 1 0 0 6.22 0.23 0.8065(0.0111) 0.0502(0.0017) 1.003 gms added Obs esd Calc Delta per gm Ia/Ir Ia/Ir Ia/Ir Ia/Ir 0.0000 0.0490 0.0011 0.0502 0.0012 0.1001 0.1336 0.0012 0.1309 -0.0026 0.1990 0.2100 0.0015 0.2107 0.0008 0.3004 0.2915 0.0017 0.2925 0.0010 AMORPH AREA 1 QUARTZ 1 0 1 5.26 0.73 0.1811(0.0077) 0.0095(0.0013) 1.007 gms added Obs esd Calc Delta per gm Ia/Ir Ia/Ir Ia/Ir Ia/Ir 0.0000 0.0091 0.0002 0.0095 0.0005 0.1001 0.0277 0.0002 0.0277 0.0000 0.1990 0.0476 0.0002 0.0456 -0.0020 0.3004 0.0623 0.0002 0.0639 0.0017 AMORPH AREA 2 QUARTZ 1 0 1 4.17 0.13 0.3306(0.0027) 0.0138(0.0004) 1.003 gms added Obs esd Calc Delta per gm Ia/Ir Ia/Ir Ia/Ir Ia/Ir 0.0000 0.0136 0.0002 0.0138 0.0002 0.1001 0.0470 0.0002 0.0469 -0.0001 0.1990 0.0802 0.0002 0.0796 -0.0007 0.3004 0.1124 0.0003 0.1131 0.0007 AMORPH AREA 3 QUARTZ 1 0 1 6.19 0.25 0.1605(0.0023) 0.0099(0.0004) 1.001 gms added Obs esd Calc Delta per gm Ia/Ir Ia/Ir Ia/Ir Ia/Ir 0.0000 0.0097 0.0002 0.0099 0.0002 0.1001 0.0265 0.0002 0.0260 -0.0005 0.1990 0.0414 0.0003 0.0419 0.0004 0.3004 0.0582 0.0003 0.0581 -0.0001 Average and weighted average for each analyte lines: Analyte Line Reference Line Average Root Mean Waverage Weighted Weighted # of Phase h k l Name h k l Wt % Square Dev. Wt % e.s.d. rms dev. Analyses AMORPH AREA 1 all all 5.23 0.03 5.23 0.53 0.02 2 AMORPH AREA 2 all all 4.16 0.01 4.16 0.11 0.01 2 AMORPH AREA 3 all all 6.21 0.02 6.21 0.17 0.02 2 Overall average and weighted average: Analyte Line Reference Line Average Root Mean Waverage Weighted Weighted # of Phase h k l Name h k l Wt % Square Dev. Wt % e.s.d. rms dev. Analyses AMORPH all all all 5.20 0.92 4.75 0.09 0.45 6 $