Phase no.: 1 3-aminoquinolin 52 reflections, N&T: 0 300.00 Code h k l Mult D(A) 2T HW Iobs Icalc Io-Ic 1 1 1 0 4 6.6159 9.969 0.023 15.1 14.9 0.2 1 1 0 1 4 6.5554 10.061 0.024 2.4 2.4 0.0 1 2 0 0 2 6.3650 10.363 0.024 80.8 79.9 0.9 1 0 1 1 4 5.4413 12.129 0.029 7.6 7.5 0.1 1 1 1 1 8 5.0034 13.195 0.032 299.1 295.7 3.5 1 2 1 0 4 4.9172 13.427 0.032 3.6 3.6 0.0 1 2 0 1 4 4.8922 13.496 0.032 13.7 13.5 0.2 1 2 1 1 8 4.1360 15.978 0.038 146.6 144.9 1.8 1 0 2 0 2 3.8719 17.076 0.041 77.0 76.0 1.0 1 0 0 2 2 3.8237 17.293 0.042 0.0 0.0 0.0 1 3 1 0 4 3.7213 17.773 0.043 5.1 5.0 0.1 1 3 0 1 4 3.7104 17.825 0.043 12.5 12.3 0.1 1 1 2 0 4 3.7044 17.854 0.043 92.7 91.5 1.2 1 1 0 2 4 3.6620 18.062 0.043 0.5 0.5 0.0 1 0 2 1 4 3.4544 19.158 0.046 49.6 48.9 0.6 1 0 1 2 4 3.4285 19.304 0.046 0.0 0.0 0.0 1 3 1 1 8 3.3461 19.784 0.048 4.0 3.9 0.0 1 1 2 1 8 3.3338 19.858 0.048 106.5 105.1 1.4 1 1 1 2 8 3.3105 19.999 0.048 6.9 6.9 0.1 1 2 2 0 4 3.3079 20.015 0.048 4.6 4.5 0.1 1 2 0 2 4 3.2777 20.201 0.049 5.5 5.4 0.1 1 4 0 0 2 3.1825 20.812 0.050 8.9 8.8 0.1 1 2 2 1 8 3.0361 21.828 0.052 78.8 77.8 1.1 1 2 1 2 8 3.0185 21.957 0.053 1.0 1.0 0.0 1 4 1 0 4 2.9436 22.523 0.054 0.3 0.3 0.0 1 4 0 1 4 2.9382 22.565 0.054 1.1 1.1 0.0 1 3 2 0 4 2.8602 23.189 0.056 10.4 10.3 0.1 1 3 0 2 4 2.8406 23.351 0.056 10.0 9.9 0.1 1 4 1 1 8 2.7471 24.157 0.058 9.0 8.9 0.1 1 0 2 2 4 2.7206 24.396 0.058 0.4 0.4 0.0 1 3 2 1 8 2.6789 24.782 0.059 11.3 11.1 0.2 1 3 1 2 8 2.6668 24.896 0.060 12.1 11.9 0.2 1 1 2 2 8 2.6606 24.955 0.060 7.0 6.9 0.1 1 1 3 0 4 2.5298 26.268 0.063 0.6 0.6 0.0 1 2 2 2 8 2.5017 26.568 0.064 1.1 1.1 0.0 1 1 0 3 4 2.4995 26.592 0.064 0.9 0.9 0.0 1 4 2 0 4 2.4586 27.043 0.065 0.0 0.0 0.0 1 4 0 2 4 2.4461 27.184 0.065 6.9 6.8 0.1 1 0 3 1 4 2.4457 27.188 0.065 8.1 8.0 0.1 1 0 1 3 4 2.4213 27.467 0.066 0.0 0.0 0.0 1 5 1 0 4 2.4186 27.498 0.066 0.8 0.8 0.0 1 5 0 1 4 2.4156 27.533 0.066 0.9 0.9 0.0 1 1 3 1 8 2.4018 27.695 0.066 13.7 13.5 0.2 1 2 3 0 4 2.3921 27.810 0.066 0.3 0.3 0.0 1 1 1 3 8 2.3787 27.970 0.067 1.9 1.8 0.0 1 2 0 3 4 2.3664 28.118 0.067 0.0 0.0 0.0 1 4 2 1 8 2.3406 28.434 0.068 0.0 0.0 0.0 1 4 1 2 8 2.3325 28.535 0.068 0.5 0.5 0.0 1 5 1 1 8 2.3060 28.869 0.069 7.2 7.1 0.1 1 3 2 2 8 2.2903 29.072 0.069 2.4 2.4 0.0 1 2 3 1 8 2.2830 29.167 0.070 0.5 0.5 0.0 1 2 1 3 8 2.2631 29.430 0.070 5.3 5.2 0.1